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题名: Preparation of Enantioenriched gamma-Substituted Lactones via Asymmetric Transfer Hydrogenation of beta-Azidocyclopropane Carboxylates Using the Ru-TsDPEN Complex
作者: Su, Y; Tu, YQ(涂永强); Gu, PM
收录类别: SCIE ; PubMed ; MEDLINE ; BIOSIS
出版日期: 2014-08-14
刊名: ORGANIC LETTERS
卷号: 16, 期号:16, 页码:4204-4207
出版者: AMER CHEMICAL SOC
出版地: WASHINGTON
英文摘要: The asymmetric transfer hydrogenation of racemic beta-azidocyclopropane carboxylates has been explored. Ru-TsDPEN B is found to be a good catalyst for the formation of enantioenriched gamma-lactones through a four-step sequence of azide reduction/cyclopropane ring cleavage/ketone transfer hydrogenation/lactonization, and the enantiomeric excess of the lactones was up to 94%.
作者部门: [Su, Yan ; Tu, Yong-Qiang] Lanzhou Univ, Dept Chem, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China ; [Su, Yan ; Gu, Peiming] Ningxia Univ, State Key Lab Cultivat Base Nat Gas Convers, Key Lab Energy Sources & Engn, Yinchuan 750021, Peoples R China ; [Su, Yan ; Gu, Peiming] Ningxia Univ, Dept Chem, Yinchuan 750021, Peoples R China
通讯作者: Tu, YQ (reprint author), Lanzhou Univ, Dept Chem, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China.
学科分类: Chemistry
文章类型: Article
所属项目编号: National Natural Science Foundation of China [21262024] ; Program for New Century Excellent Talents in University [NCET-13-0874] ; Scientific Research Foundation for Returned Scholars (Ministry of Education of China)
所属项目名称: 国家自然科学基金项目 ; 新世纪优秀人才支持计划
项目资助者: NSFC ; MOE
语种: 英语
DOI: 10.1021/ol501895k
ISSN号: 1523-7060
WOS记录号: WOS:000340517200038
PM记录号: 25083937
BIOSIS记录号: BIOSIS:PREV201400658344
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内容类型: 期刊论文
URI标识: http://ir.lzu.edu.cn/handle/262010/103051
Appears in Collections:化学化工学院_期刊论文

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Recommended Citation:
Su, Y,Tu, YQ,Gu, PM. Preparation of Enantioenriched gamma-Substituted Lactones via Asymmetric Transfer Hydrogenation of beta-Azidocyclopropane Carboxylates Using the Ru-TsDPEN Complex[J]. ORGANIC LETTERS,2014,16(16):4204-4207.
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