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题名: CONVERGENT AND STEREOSELECTIVE SYNTHESIS OF SARCOPHYTOL-Q PRECURSOR - (11S)-3,7,11,15-TETRAMETHYL-11-HYDROXY-L4-OXO-3E,7E,12E-HEXADECATRIENAL
作者: LI, WD; Li, YL(李裕林); Li, Y(李瀛)
收录类别: SCIE
出版日期: 1995-08-01
会议名称: 3rd International Symposium for Chinese Organic Chemists (ISCOC 94 TAIPEI)
会议日期: NOV 10-13, 1994
会议地点: TAIPEI, TAIWAN
英文摘要: A chiral precursor of sarcophytol-Q, (11S)-3,7,11,15-tetramethyl-11-hydroxy-14-oxo-3E,7E,12E-hexadecatrienal, was synthesized in a convergent and stereoselective manner starting from geraniol and 4-hydroxy-2-butanone in nine steps. The key steps were asymmetric Sharpless epoxidation, base-induced dehydrohalogenation rearrangement of chiral epoxy chloride 5 and the phase transfer catalytic coupling reaction of allylic phenyl sulfone 4 with chiral allylic chloride 3.
关键词: MACROCYCLIC DITERPENOIDS ; SARCOPHYTOL-Q ; PRECURSOR ; SYNTHESIS
作者部门: LANZHOU UNIV,INST ORGAN CHEM,LANZHOU 730000,PEOPLES R CHINA
通讯作者: LI, WD (reprint author), NANKAI UNIV,STATE KEY LAB ELEMENTOORGAN CHEM,TIANJIN 300071,PEOPLES R CHINA.
学科分类: Chemistry
会议录: JOURNAL OF THE CHINESE CHEMICAL SOCIETY
期号: 4
页码: 701-707
出版者: CHINESE CHEM SOC
出版地: TAIPEI
语种: 英语
ISSN号: 0009-4536
WOS记录号: WOS:A1995RN66300014
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内容类型: 会议论文
URI标识: http://ir.lzu.edu.cn/handle/262010/113137
Appears in Collections:化学化工学院_会议论文

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Recommended Citation:
LI, WD,LI, YL,LI, Y. CONVERGENT AND STEREOSELECTIVE SYNTHESIS OF SARCOPHYTOL-Q PRECURSOR - (11S)-3,7,11,15-TETRAMETHYL-11-HYDROXY-L4-OXO-3E,7E,12E-HEXADECATRIENAL[C]. 见:3rd International Symposium for Chinese Organic Chemists (ISCOC 94 TAIPEI). TAIPEI, TAIWAN. NOV 10-13, 1994.
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