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题名: Convenient synthesis of (S)-alpha,alpha'-diphenyl-2-pyrrolidinemethanol
其他题名: (S)-α,α’-二苯基-2-吡咯烷甲醇的简便合成
作者: Yang, XW; Ni, JM(倪京满); Wang, R(王锐); Pan, XF(潘鑫复)
收录类别: SCIE ; CSCD
出版日期: 1997-06
刊名: CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
卷号: 18, 期号:6, 页码:911-913
期刊主办单位: 吉林大学
出版者: HIGHER EDUCATION PRESS
出版地: BEIJING
英文摘要: A convenient synthesis of optically active alpha,alpha'-diphenyl-2-pyrrolidinemethanol(1) starting from L-proline, based on different N-protections, was described. Different N-protections had no effect on the optical purity of compound 1, but gave different chemical yields. The yield was the lowest when PhCH2 was employed for N-protection. An investigation on the effect of N-protection on the chemical yield and the optical purity of compound 1 led to a convenient preparation of the new chiral oxazolidinone 3. The structure of 3 was identified with H-1 NMR, C-13 NMR, MS and IR.
关键词: synthesis ; alpha,alpha'-diphenyl-2-pyrrolidinemethanol ; oxazolidinone ; 合成,(S)-α ; α’-二苯基-2-吡咯烷甲醇 ; 唑烷酮
作者部门: LANZHOU UNIV,DEPT BIOL,STATE KEY LAB APPL ORGAN CHEM,LANZHOU 730000,PEOPLES R CHINA ; LANZHOU UNIV,DEPT CHEM,STATE KEY LAB APPL ORGAN CHEM,LANZHOU 730000,PEOPLES R CHINA
学科分类: Chemistry
文章类型: Article
所属项目编号: 国家自然科学基金 ; 国家教育委员会优秀年轻教师基金 ; 博士点基金
所属项目名称: 国家自然科学基金项目 ; 高等学校博士学科点专项科研基金
项目资助者: NSFC ; MOE
语种: 中文
ISSN号: 0251-0790
WOS记录号: WOS:A1997XU77500021
CSCD记录号: CSCD:369701
第一机构:
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内容类型: 期刊论文
URI标识: http://ir.lzu.edu.cn/handle/262010/116009
Appears in Collections:生命科学学院_期刊论文

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Recommended Citation:
Yang, XW,Ni, JM,Wang, R,et al. Convenient synthesis of (S)-alpha,alpha'-diphenyl-2-pyrrolidinemethanol[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,1997,18(6):911-913.
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