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Convenient synthesis of (S)-alpha,alpha'-diphenyl-2-pyrrolidinemethanol
其他题名(S)-α,α’-二苯基-2-吡咯烷甲醇的简便合成
Yang, XW; Ni, JM(倪京满); Wang, R(王锐); Pan, XF(潘鑫复)
收录类别SCIE ; CSCD
1997-06
发表期刊CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
卷号18期号:6页码:911-913
期刊主办单位吉林大学
出版者HIGHER EDUCATION PRESS
出版地BEIJING
摘要A convenient synthesis of optically active alpha,alpha'-diphenyl-2-pyrrolidinemethanol(1) starting from L-proline, based on different N-protections, was described. Different N-protections had no effect on the optical purity of compound 1, but gave different chemical yields. The yield was the lowest when PhCH2 was employed for N-protection. An investigation on the effect of N-protection on the chemical yield and the optical purity of compound 1 led to a convenient preparation of the new chiral oxazolidinone 3. The structure of 3 was identified with H-1 NMR, C-13 NMR, MS and IR.
关键词Synthesis Oxazolidinone Alpha Alpha'-diphenyl-2-pyrrolidinemethanol Α’-二苯基-2-吡咯烷甲醇 合成 唑烷酮 (s)-α
作者部门LANZHOU UNIV,DEPT BIOL,STATE KEY LAB APPL ORGAN CHEM,LANZHOU 730000,PEOPLES R CHINA;
LANZHOU UNIV,DEPT CHEM,STATE KEY LAB APPL ORGAN CHEM,LANZHOU 730000,PEOPLES R CHINA
学科领域Chemistry
所属项目编号国家自然科学基金 ; 国家教育委员会优秀年轻教师基金 ; 博士点基金
资助项目国家自然科学基金项目 ; 高等学校博士学科点专项科研基金
项目资助者NSFC ; MOE
ISSN0251-0790
文章类型Article
语种中文
WOS记录号WOS:A1997XU77500021
CSCD记录号CSCD:369701
第一机构
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文献类型期刊论文
条目标识符http://ir.lzu.edu.cn/handle/262010/116009
Collection生命科学学院
Recommended Citation:
GB/T 7714
Yang, XW,Ni, JM,Wang, R,et al. Convenient synthesis of (S)-alpha,alpha'-diphenyl-2-pyrrolidinemethanol[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,1997,18(6):911-913.
APA Yang, XW,Ni, JM,Wang, R,&Pan, XF.(1997).Convenient synthesis of (S)-alpha,alpha'-diphenyl-2-pyrrolidinemethanol.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,18(6),911-913.
MLA Yang, XW,et al."Convenient synthesis of (S)-alpha,alpha'-diphenyl-2-pyrrolidinemethanol".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 18.6(1997):911-913.
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