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题名: Lewis Acid Mediated Tandem Reaction of Propargylic Alcohols with Hydroxylamine Hydrochloride To Give alpha,beta-Unsaturated Amides and Alkenyl Nitriles
其他题名: Lewis Acid Mediated Tandem Reaction of Propargylic Alcohols with Hydroxylamine Hydrochloride to Give α,β-Unsaturated Amides and Alkenyl Nitriles
作者: Han, YP; Song, XR; Qiu, YF; Hao, XH; Wang, J; Wu, XX; Liu, XY(刘雪原); Liang, YM(梁永民)
收录类别: SCIE ; EI ; MEDLINE ; BIOSIS
出版日期: 2015-09-18
刊名: JOURNAL OF ORGANIC CHEMISTRY
卷号: 80, 期号:18, 页码:9200-9207
英文摘要: We have developed a highly selective method for the synthesis of alpha,beta-unsaturated amides and alkenyl nitriles from readily available propargylic alcohols. The reaction proceeded smoothly under the neutral conditions with hydroxylamine hydrochloride (NH2OH center dot HCl) as the nitrogen source. The development of these new strategies has significantly extended the application of hydroxylamine hydrochloride to the chemistry of propargylic alcohols. Moreover, both secondary and tertiary alcohols have been highly regioselectively transformed to the desired products with good functional group compatibility.
作者部门: [Han, Ya-Ping ; Song, Xian-Rong ; Qiu, Yi-Feng ; Hao, Xin-Hua ; Wang, Jia ; Wu, Xin-Xing ; Liu, Xue-Yuan ; Liang, Yong-Min] Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China
通讯作者: Liang, YM (reprint author), Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China.
学科分类: Chemistry
文章类型: Article
所属项目编号: National Science Foundation [NSF21272101, NSF21472073, NSF21472074, NSF21302076] ; Program for Changjiang Scholars and Innovative Research Team in University [IRT1138]
所属项目名称: 国家自然科学基金项目 ; 长江学者和创新团队发展计划
项目资助者: NSFC ; MOE
语种: 英语
DOI: 10.1021/acs.joc.5b01633
ISSN号: 0022-3263
WOS记录号: WOS:000361866700029
EI记录号: 20153901300720
PM记录号: 26317753
BIOSIS记录号: BCI:BCI201500766919
IR记录号: WOS:000361866700029
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内容类型: 期刊论文
URI标识: http://ir.lzu.edu.cn/handle/262010/180177
Appears in Collections:化学化工学院_期刊论文

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Recommended Citation:
Han, YP,Song, XR,Qiu, YF,et al. Lewis Acid Mediated Tandem Reaction of Propargylic Alcohols with Hydroxylamine Hydrochloride To Give alpha,beta-Unsaturated Amides and Alkenyl Nitriles[J]. JOURNAL OF ORGANIC CHEMISTRY,2015,80(18):9200-9207.
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