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兰州大学机构库  > 化学化工学院  > 期刊论文
题名: NH4HF2 as a Selective TBS-Removal Reagent for the Synthesis of Highly Functionalized Spiroketal via Tandem Deprotection/Spiroketalization Procedure
作者: Lu, H; Zhang, FM(张辅民); Pan, JL; Chen, T; Li, YF(李彦锋)
收录类别: SCIE ; PubMed ; MEDLINE ; BIOSIS
出版日期: 2014-01-17
刊名: JOURNAL OF ORGANIC CHEMISTRY
卷号: 79, 期号:2
出版者: AMER CHEMICAL SOC
出版地: WASHINGTON
英文摘要: NH4HF2 has been used for the first time to selectively remove the TBS protecting groups from diol ketone precursors in the synthesis of highly functionalized spiroketals. This method allows the synthesis of [5,6], [6,6], and [6,7] spiroketal skeletons, as well as benzannulated spiroketal with retention of acid-sensitive groups. In this way, spiroketals can be synthesized with diverse substituent groups in the skeleton or on side chains. To demonstrate the utility of this methodology, the diverse transformations of highly functionalized spiroketal 3f were also investigated.
作者部门: [Zhang, Fu-Min] Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China ; Lanzhou Univ, Dept Chem, Lanzhou 730000, Peoples R China
通讯作者: Zhang, FM (reprint author), Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China.
学科分类: Chemistry
文章类型: Article
所属项目编号: NSFC [21272097, 21290181] ; "111"Program ; PCSIRT of MOE [IRT1138]
所属项目名称: 国家自然科学基金项目 ; 长江学者和创新团队发展计划
项目资助者: NSFC ; MOE
语种: 英语
DOI: 10.1021/jo402167q
ISSN号: 0022-3263
WOS记录号: WOS:000330099000009
PM记录号: 24328167
BIOSIS记录号: BIOSIS:PREV201400192392
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内容类型: 期刊论文
URI标识: http://ir.lzu.edu.cn/handle/262010/75420
Appears in Collections:化学化工学院_期刊论文

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Recommended Citation:
Lu, H; Zhang, FM; Pan, JL; Chen, T; Li, YF.NH4HF2 as a Selective TBS-Removal Reagent for the Synthesis of Highly Functionalized Spiroketal via Tandem Deprotection/Spiroketalization Procedure,JOURNAL OF ORGANIC CHEMISTRY,2014,79(2):
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